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dc.contributor.authorAl-Ithawi, W. K. A.en
dc.contributor.authorAl-Sammarraie, E. S. A.en
dc.contributor.authorBaklykov, A. V.en
dc.contributor.authorPlatonov, V. A.en
dc.contributor.authorAltobee, A. M. K.en
dc.contributor.authorGlebov, N. S.en
dc.contributor.authorKhasanov, A. F.en
dc.contributor.authorKovalev, I. S.en
dc.contributor.authorNikonov, I. L.en
dc.contributor.authorKopchuk, D. S.en
dc.contributor.authorZyryanov, G. V.en
dc.date.accessioned2025-12-18T07:11:02Z-
dc.date.available2025-12-18T07:11:02Z-
dc.date.issued2024-
dc.identifier.citationMechanosynthesis of pentiptycene-based polyesters and polycarbonates / W. K. A. Al-Ithawi, E. S. A. Al-Sammarraie, A. V. Baklykov [et al.] // Chimica Techno Acta. – 2024. – Vol. 11. – Iss. 3. – № 202411306. DOI: 10.15826/chimtech.2024.11.3.06.en
dc.identifier.citationAl-Ithawi, W. A. K., Al-Sammarraie, E. S. A., Baklykov, A. V., Platonov, V. A., Altobee, A. M. K., Glebov, N. S., … Zyryanov, G. V. (2024). Mechanosynthesis of pentiptycene-based polyesters and polycarbonates. Chimica Techno Acta, 11(3). doi:10.15826/chimtech.2024.11.3.06apa
dc.identifier.issn2409-5613-
dc.identifier.otherhttps://journals.urfu.ru/index.php/chimtech/article/download/7716/5649pdf
dc.identifier.urihttps://elar.usfeu.ru/handle/123456789/14548-
dc.description.abstractIptycenes are common building blocks for the small-molecules or polymer-based chemosensors and fluorophores. In addition, iptycene derivatives are widely presented in polymers of intrinsic microporosity (PIMs) as materials for the separation and purification technologies. In this manuscript we wish to report a mechanochemical approach to pentiptycene-based polyesters and polycarbonates as, possibly, new representatives of PIMs. Our approach involves the polycondensation reaction between 5,7,12,14-tetrahydro-5,14:7,12-bis([1,2]benzeno)pentacene-6,13-diol (pentiptycene-6,13-diol) and triphosgene or oxalyl chloride under ball-milling conditions. The obtained polymers were characterized by means of 1H NMR- and IR-spectroscopy. As the last step, the fluorescence “turn-off” response of pentiptycene-6,13-diol and two pentiptycene-based polymers towards nitroanalytes (2,4-dinitrotioluene (DNT) and 2,4,6-trinitrophenole (picric acid, PA)) was investigated, and Stern-Volmer constants as high as 1o4 M–1 were observed. © 2024, the Authors.en
dc.description.sponsorshipUral Branch, Russian Academy of Sciences, UB RAS; Ministry of Education and Science of the Russian Federation, Minobrnauka, (075-15-2022-1118, 29.06.2022); Ministry of Education and Science of the Russian Federation, Minobrnaukaen
dc.description.sponsorshipFunding text 1: The authors are thankful to the Ministry of Science and Higher Education of the Russian Federation (Agreement # 075-15-2022-1118 dated 29.06.2022), http://www.minobrnauki.gov.ru. This work was performed using the equipment of the Joint Use Center "Spectroscopy and Analysis of Organic Compounds" of the I. Ya. Postovsky Institute of Organic Synthesis of the Ural Branch of the Russian Academy of Sciences.; Funding text 2: The authors are thankful to the Ministry of Science and Higher Education of the Russian Federation (Agreement # 075-15-2022-1118 dated 29.06.2022), http://www.minobr-en
dc.format.mimetypeapplication/pdfen
dc.language.isoenen
dc.publisherUral Federal Universityen
dc.rightsinfo:eu-repo/semantics/openAccessen
dc.sourceChimica Techno Actaen
dc.subjectDETECTION OF NITROANALYTESen
dc.subjectMECHANOSYNTHESISen
dc.subjectPENTIPTYCENEen
dc.subjectPOLYCARBONATEen
dc.subjectPOLYESTERen
dc.subjectPOROUS POLYMERSen
dc.titleMechanosynthesis of pentiptycene-based polyesters and polycarbonatesen
dc.typeArticleen
dc.typeinfo:eu-repo/semantics/articleen
dc.typeinfo:eu-repo/semantics/publishedVersionen
local.issue3-
local.volume11-
local.identifier.doi10.15826/chimtech.2024.11.3.06-
local.affiliationInstitute of Chemical Engineering, Yekaterinburg, Sverdlovskaya, Russian Federationen
local.affiliationUniversity of Technology- Iraq, Baghdad, Baghdad, Iraqen
local.affiliationPostovsky Institute of Organic Synthesis of Ural Division of Russian Academy of Sciences, Yekaterinburg, Sverdlovskaya, Russian Federationen
local.affiliationUral State Forest Engineering University, Yekaterinburg, Sverdlovskaya, Russian Federationen
local.contributor.employeeAl-Ithawi, Wahab K.A., Institute of Chemical Engineering, Yekaterinburg, Sverdlovskaya, Russian Federation, University of Technology- Iraq, Baghdad, Baghdad, Iraqen
local.contributor.employeeAl-Sammarraie, Eman S.A., Institute of Chemical Engineering, Yekaterinburg, Sverdlovskaya, Russian Federation, University of Technology- Iraq, Baghdad, Baghdad, Iraqen
local.contributor.employeeBaklykov, Artem V., Institute of Chemical Engineering, Yekaterinburg, Sverdlovskaya, Russian Federation, Postovsky Institute of Organic Synthesis of Ural Division of Russian Academy of Sciences, Yekaterinburg, Sverdlovskaya, Russian Federationen
local.contributor.employeePlatonov, Vadim A., Institute of Chemical Engineering, Yekaterinburg, Sverdlovskaya, Russian Federationen
local.contributor.employeeAltobee, Aqeel M.K., Institute of Chemical Engineering, Yekaterinburg, Sverdlovskaya, Russian Federationen
local.contributor.employeeGlebov, Nikita S., Institute of Chemical Engineering, Yekaterinburg, Sverdlovskaya, Russian Federationen
local.contributor.employeeKhasanov, Albert F., Institute of Chemical Engineering, Yekaterinburg, Sverdlovskaya, Russian Federationen
local.contributor.employeeKovalev, Igor S., Institute of Chemical Engineering, Yekaterinburg, Sverdlovskaya, Russian Federationen
local.contributor.employeeNikonov, Igor L., Institute of Chemical Engineering, Yekaterinburg, Sverdlovskaya, Russian Federation, Postovsky Institute of Organic Synthesis of Ural Division of Russian Academy of Sciences, Yekaterinburg, Sverdlovskaya, Russian Federation, Ural State Forest Engineering University, Yekaterinburg, Sverdlovskaya, Russian Federationen
local.contributor.employeeKopchuk, Dmitry S., Institute of Chemical Engineering, Yekaterinburg, Sverdlovskaya, Russian Federation, Postovsky Institute of Organic Synthesis of Ural Division of Russian Academy of Sciences, Yekaterinburg, Sverdlovskaya, Russian Federationen
local.contributor.employeeZyryanov, Grigory V., Institute of Chemical Engineering, Yekaterinburg, Sverdlovskaya, Russian Federation, Postovsky Institute of Organic Synthesis of Ural Division of Russian Academy of Sciences, Yekaterinburg, Sverdlovskaya, Russian Federationen
local.identifier.rsi72799324-
local.identifier.eid2-s2.0-85201220662-
local.description.order202411306-
local.identifier.ednFECLEY-
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